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Beilstein J. Org. Chem. 2015, 11, 2158–2165, doi:10.3762/bjoc.11.233
Graphical Abstract
Scheme 1: Traditional activating mode and oxidative activation mode of free carboxylic acids in amide formati...
Scheme 2: Substrate scope for catalytic, direct amide formation from carboxylic acids and azoles. Reaction co...
Scheme 3: Further investigation into the scope of amine.
Scheme 4: Possible transamidation process.
Scheme 5: Scope of the amine transamidation from benzimidazole amides. Reaction conditions: benzimidazole ami...
Scheme 6: Preparative scale of the reaction.
Scheme 7: Radical scavenger reaction.
Scheme 8: Control reactions.
Scheme 9: Proposed mechanism.